PASCO Specialty & Mfg. CI-6734 User Manual Page 17

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012–06615A Sodium Ion Selective Electrode
13
Standards & Reagents
Whenever problems arise with the measuring procedure that has been used successfully in the past, be Sure to check
the standard and reagent solutions. If in doubt about the credibility of any of the solutions, prepare them again. Errors
may result from contamination of the ISA, incorrect dilution of standards, poor quality distilled/deionized water,
or a simple mathematical miscalculation.
Sample
Look for possible interferences, complexing agents, or substances which could affect the response or physically
damage the sensing electrode (or the reference electrode) if the electrodes work perfectly in the standard, but not
in the sample.
Try to determine the composition of the samples prior to testing to eliminate a problem before it starts. (See
Measuring Hints, Sample Requirements, and Interferences.)
Technique
Be sure that the electrode’s limit of detection has not been exceeded. Be sure that the analysis method is clearly
understood and is compatible with the sample.
Refer to the instruction manual again. Reread General Preparation and Electrode Characteristics.
If trouble still persists, call PASCO Technical Support.
Troubleshooting Hints
Symptom Possible Causes Next Step
Out of Range Reading defective electrode check electrode operation
electrodes not plugged in unplug electrodes and reseat electrodes
properly
reference electrode not filled replenish reference filling solution
electrodes not in solution put electrodes in solution
air bubble on membrane remove bubble by re-dipping electrode
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